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Non-Volatile Glycerin Gel Enhanced by Sub-5 nm Particles with Super Elasticity, Recoverability, and High Temperature Resistance
Li,Lefan1; Wang,Qiao1; Li,Zongjin1; Guo,Siyao2; Sun,Guoxing1
2019-02
Source PublicationMacromolecular Chemistry and Physics
ISSN1022-1352
Volume220Issue:4
Abstract

A gel material that can be applied to industry needs to fulfill two requirements: excellent mechanical properties and high temperature resistance. Previous research developed a hydrogel enhanced by sub-5 nm particles, with excellent mechanical properties. While its application in the open environment is still limited by the volatilization of inner moisture, in this research, a non-volatile gel (NV gel) enhanced by 5-nm spherulites is manufactured. The NV gel remains stable after staying at 90 °C for 24 h. Meanwhile, being enhanced by sub-5 nm nanospherulites, the NV gel shows good mechanical properties: with 200 ppm nanoparticle content, the tensile strength reaches 814 kPa and the compressive stress is 173.41 MPa at a recoverable 99% strain. The high temperature resistance is characterized by thermogravimetric analysis (TGA) and mechanical testing after thermal treatment. Transmission electron microscopy, scanning electron microscopy, Fourier transform infrared spectroscopy, time of flight secondary ion mass spectrometry, and thermogravimetric analysis are used to evaluate the microstructure of NV gel. Possessing non-volatile and good mechanical properties at the same time, this NV gel becomes very suitable for fulfilling the application requirement as an engineering material.

KeywordHigh Temperature Resistance Mechanical Properties Nanocomposites Non-volatile Gels
DOI10.1002/macp.201800464
URLView the original
Indexed BySCIE
Language英語English
WOS Research AreaPolymer Science
WOS SubjectPolymer Science
WOS IDWOS:000459018900007
PublisherWILEY-V C H VERLAG GMBH, POSTFACH 101161, 69451 WEINHEIM, GERMANY
Scopus ID2-s2.0-85059661041
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Cited Times [WOS]:2   [WOS Record]     [Related Records in WOS]
Document TypeJournal article
CollectionUniversity of Macau
Corresponding AuthorGuo,Siyao; Sun,Guoxing
Affiliation1.Joint Key Laboratory of the Ministry of Education,Institute of Applied Physics and Materials Engineering,University of MacauAvenida da Universidade,Taipa,999078,Taiwan
2.School of Civil EngineeringQingdao Technological University,Qingdao,266033,China
First Author AffilicationINSTITUTE OF APPLIED PHYSICS AND MATERIALS ENGINEERING
Corresponding Author AffilicationINSTITUTE OF APPLIED PHYSICS AND MATERIALS ENGINEERING
Recommended Citation
GB/T 7714
Li,Lefan,Wang,Qiao,Li,Zongjin,et al. Non-Volatile Glycerin Gel Enhanced by Sub-5 nm Particles with Super Elasticity, Recoverability, and High Temperature Resistance[J]. Macromolecular Chemistry and Physics,2019,220(4).
APA Li,Lefan,Wang,Qiao,Li,Zongjin,Guo,Siyao,&Sun,Guoxing.(2019).Non-Volatile Glycerin Gel Enhanced by Sub-5 nm Particles with Super Elasticity, Recoverability, and High Temperature Resistance.Macromolecular Chemistry and Physics,220(4).
MLA Li,Lefan,et al."Non-Volatile Glycerin Gel Enhanced by Sub-5 nm Particles with Super Elasticity, Recoverability, and High Temperature Resistance".Macromolecular Chemistry and Physics 220.4(2019).
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