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Synthesis of AlPO 4 -5 crystals using TBAOH as template
Jiang F.Y.1; Tang Z.K.3; Zhai J.P.3; Ye J.T.3; Han J.R.1
2006-06-20
Source PublicationMicroporous and Mesoporous Materials
ISSN13871811
Volume92Issue:1-3Pages:129-133
AbstractWe report the hydrothermal synthesis of AlPO -5 crystals using TBAOH as template. The resulting product sensitively depends on the gel compositions and synthesis procedure. By treating the tri-isopropylate aluminum gel solution with ultrasonic, and adding HF acid to adjust the gel pH value, perfect hexagonal-shaped AlPO -5 crystals are obtained. At high TBAOH content, some centrosymmetric intersecting crystals are observed in the products, this can be interpreted by the polar growth of AlPO -5 crystals. The decomposition of template TBAOH in the channels of AlPO -5 crystals has been studied by FTIR and TG analysis. © 2006 Elsevier Inc. All rights reserved.
KeywordAlPO 4 -5 Crystal morphology Organic template Polar growth Ultrasonic
DOI10.1016/j.micromeso.2005.12.021
URLView the original
Language英語English
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Cited Times [WOS]:23   [WOS Record]     [Related Records in WOS]
Document TypeJournal article
CollectionUniversity of Macau
Affiliation1.Shandong University
2.Yantai University
3.Hong Kong University of Science and Technology
Recommended Citation
GB/T 7714
Jiang F.Y.,Tang Z.K.,Zhai J.P.,et al. Synthesis of AlPO 4 -5 crystals using TBAOH as template[J]. Microporous and Mesoporous Materials,2006,92(1-3):129-133.
APA Jiang F.Y.,Tang Z.K.,Zhai J.P.,Ye J.T.,&Han J.R..(2006).Synthesis of AlPO 4 -5 crystals using TBAOH as template.Microporous and Mesoporous Materials,92(1-3),129-133.
MLA Jiang F.Y.,et al."Synthesis of AlPO 4 -5 crystals using TBAOH as template".Microporous and Mesoporous Materials 92.1-3(2006):129-133.
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