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Preparative Separation of Patchouli Alcohol from Patchouli Oil Using High Performance Centrifugal Partition Chromatography
Li X.-C.2; Zhang Q.-W.2; Yin Z.-Q.3; Zhang X.-Q.1; Ye W.-C.1
2011
Source PublicationJournal of Essential Oil Research
ISSN10412905
Volume23Issue:6Pages:19-24
Abstract

A high-performance centrifugal partition chromatography (HPCPC) method was developed for the preparative separation of patchouli alcohol. The separation was performed with a nonaqueous two-phase solvent system consisting of petroleum ether (bp.30–60°C)-acetonitrile (1:1, v/v) in descending separation mode. A total of more than 2 g of patchouli alcohol was isolated from the essential oil (12.5 g) in 300 min. This component was separated and identified by comparing its retention time and MS data with the standard substance analyzed by GC/MS. The purity was more than 98%. About 450 mL petroleum ether and 550 mL acetonitrile were used for a single run, and 60% and 80% of petroleum ether and acetonitrile could be recovered for next run, respectively.

KeywordHigh-performance Centrifugal Partition Chromatography Patchouli Patchouli Alcohol Pogostemon Cablin Preparative Separation
DOI10.1080/10412905.2011.9712276
URLView the original
Indexed BySCIE
Language英语
WOS Research AreaChemistry ; Food Science & Technology
WOS SubjectChemistry, Applied ; Food Science & Technology
WOS IDWOS:000296950100004
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Cited Times [WOS]:8   [WOS Record]     [Related Records in WOS]
Document TypeJournal article
CollectionInstitute of Chinese Medical Sciences
Affiliation1.Jinan University
2.Universidade de Macau
3.China Pharmaceutical University
Recommended Citation
GB/T 7714
Li X.-C.,Zhang Q.-W.,Yin Z.-Q.,et al. Preparative Separation of Patchouli Alcohol from Patchouli Oil Using High Performance Centrifugal Partition Chromatography[J]. Journal of Essential Oil Research,2011,23(6):19-24.
APA Li X.-C.,Zhang Q.-W.,Yin Z.-Q.,Zhang X.-Q.,&Ye W.-C..(2011).Preparative Separation of Patchouli Alcohol from Patchouli Oil Using High Performance Centrifugal Partition Chromatography.Journal of Essential Oil Research,23(6),19-24.
MLA Li X.-C.,et al."Preparative Separation of Patchouli Alcohol from Patchouli Oil Using High Performance Centrifugal Partition Chromatography".Journal of Essential Oil Research 23.6(2011):19-24.
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