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Quantitative analysis of six polyynes and one polyene in Oplopanax horridus and Oplopanax elatus by pressurized liquid extraction and on-line SPE-HPLC
Huang W.2; Yang J.2; Zhao J.2; Wang C.-Z.1; Yuan C.-S.1; Li S.-P.2
2010-12-01
Source PublicationJournal of Pharmaceutical and Biomedical Analysis
ISSN07317085
Volume53Issue:4Pages:906-910
Abstract

A pressurized liquid extraction and on-line SPE-HPLC method was developed for simultaneous determination of six polyynes, including falcarindiol, oplopandiol, (11S,16S,9Z)-9,17-octadecadiene-12,14-diyne-1,11,16-triol,1-acetate, oplopandiol acetate, oplopantriol A, oplopantriol B, and one polyene, (S,E)-nerolidol, in Oplopanax horridus and Oplpanax elatus. The analysis was conducted on a Grace Prevail C column (3μm, 7mm×33mm) with gradient elution of acetonitrile and water after the sample loaded and washed with 42%ACN in 0.3min on a phenomenex Strata-X on-line Extraction Cartridge SPE column (2.5μm, 2.0×20mm). All calibration curves of seven analytes showed good linearity within the test ranges. The validated method was successfully applied to quantify six polyynes and one polyene in two species of Oplopanax, O. horridus and O. elatus. © 2010 Elsevier B.V.

KeywordOplopanax Polyene Polyynes Pressurized Liquid Extraction Spe-hplc
DOI10.1016/j.jpba.2010.06.021
URLView the original
Indexed BySCI
WOS Research AreaChemistry ; Pharmacology & Pharmacy
WOS SubjectChemistry, Analytical ; Pharmacology & Pharmacy
WOS IDWOS:000281334500012
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Cited Times [WOS]:13   [WOS Record]     [Related Records in WOS]
Document TypeJournal article
CollectionInstitute of Chinese Medical Sciences
Affiliation1.University of Chicago Pritzker School of Medicine
2.University of Macau
First Author AffilicationUniversity of Macau
Recommended Citation
GB/T 7714
Huang W.,Yang J.,Zhao J.,et al. Quantitative analysis of six polyynes and one polyene in Oplopanax horridus and Oplopanax elatus by pressurized liquid extraction and on-line SPE-HPLC[J]. Journal of Pharmaceutical and Biomedical Analysis,2010,53(4):906-910.
APA Huang W.,Yang J.,Zhao J.,Wang C.-Z.,Yuan C.-S.,&Li S.-P..(2010).Quantitative analysis of six polyynes and one polyene in Oplopanax horridus and Oplopanax elatus by pressurized liquid extraction and on-line SPE-HPLC.Journal of Pharmaceutical and Biomedical Analysis,53(4),906-910.
MLA Huang W.,et al."Quantitative analysis of six polyynes and one polyene in Oplopanax horridus and Oplopanax elatus by pressurized liquid extraction and on-line SPE-HPLC".Journal of Pharmaceutical and Biomedical Analysis 53.4(2010):906-910.
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