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Optimization and comparison of three methods for extraction of volatile compounds from Cyperus rotundus evaluated by gas chromatography-mass spectrometry
Tam C.U.; Yang F.Q.; Zhang Q.W.; Guan J.; Li S.P.
2007
Source PublicationJournal of Pharmaceutical and Biomedical Analysis
ISSN7317085
Volume44Issue:2Pages:444
Abstract

The essential oil of Cyperus rotundus has multiple pharmacological activities. Therefore, the extraction with high yield and quality is very important for preparation of essential oil of C. rotundus. In this paper, three methods, namely hydrodistillation (HD), pressurized liquid extraction (PLE) and supercritical fluid extraction (SFE), for extraction of volatile compounds from C. rotundus were optimized and compared by gas chromatography-mass spectrometry. Among eight identified compounds in C. rotundus, five components including α-copaene, cyperene, β-selinene, β-cyperone and α-cyperone were quantitatively determined or estimated using α-cyperone as standard, which showed that PLE had the highest extraction efficiency, while SFE had the best selectivity for extraction of β-cyperone and α-cyperone. The contents of ingredients from C. rotundus extracted with HD, PLE and SFE are significantly different, which suggest that comparison of chemical components and pharmacological activities of different extracts is helpful to elucidate the active components in C. rotundus and control its quality.

KeywordCyperus Rotundus Gas Chromatography-mass Spectrometry Hydrodistillation Pressurized Liquid Extraction Supercritical Fluid Extraction
DOI10.1016/j.jpba.2006.10.026
URLView the original
Indexed BySCIE
Language英语
WOS Research AreaChemistry ; Pharmacology & Pharmacy
WOS SubjectChemistry, Analytical ; Pharmacology & Pharmacy
WOS IDWOS:000247765400015
The Source to ArticleScopus
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Cited Times [WOS]:30   [WOS Record]     [Related Records in WOS]
Document TypeJournal article
CollectionInstitute of Chinese Medical Sciences
Corresponding AuthorLi S.P.
AffiliationInstitute of Chinese Medical Sciences, University of Macau, Taipa, Macau SAR, China
First Author AffilicationInstitute of Chinese Medical Sciences
Corresponding Author AffilicationInstitute of Chinese Medical Sciences
Recommended Citation
GB/T 7714
Tam C.U.,Yang F.Q.,Zhang Q.W.,et al. Optimization and comparison of three methods for extraction of volatile compounds from Cyperus rotundus evaluated by gas chromatography-mass spectrometry[J]. Journal of Pharmaceutical and Biomedical Analysis,2007,44(2):444.
APA Tam C.U.,Yang F.Q.,Zhang Q.W.,Guan J.,&Li S.P..(2007).Optimization and comparison of three methods for extraction of volatile compounds from Cyperus rotundus evaluated by gas chromatography-mass spectrometry.Journal of Pharmaceutical and Biomedical Analysis,44(2),444.
MLA Tam C.U.,et al."Optimization and comparison of three methods for extraction of volatile compounds from Cyperus rotundus evaluated by gas chromatography-mass spectrometry".Journal of Pharmaceutical and Biomedical Analysis 44.2(2007):444.
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