UM
Synthesis of large silicon substituted AlPO4-11 single crystals
Fu L.2; Zhai J.P.2; Hu J.M.1; Li I.L.2; Ruan S.C.2; Tang Z.K.1
2011
Source PublicationMicroporous and Mesoporous Materials
ISSN13871811
Volume137Issue:1-3Pages:1-7
AbstractWe report the effects of gel composition and crystallization conditions on the hydrothermal synthesis of large silicon substituted AlPO-11 single crystals (SAPO-11). Perfect large SAPO-11 single crystals with a typical dimension of 40 × 80 × 180 μm were synthesized by optimizing the following synthesis conditions: crystallization temperature and duration, molar ratio SiO/AlO, amount of the organic template dipropylamine (DPA) and HF. Single-crystal X-ray diffraction measurement showed that the as-synthesized SAPO-11 single crystals are of space group Icm2 symmetry with lattice constants a = 13.384 , b = 18.60 and c = 8.414 , and their unit cell volume is V = 2094 . © 2010 Elsevier Inc. All rights reserved.
KeywordMolecular sieve SAPO-11 Single crystals Synthesis
DOI10.1016/j.micromeso.2010.08.014
URLView the original
Language英語
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Cited Times [WOS]:16   [WOS Record]     [Related Records in WOS]
Document TypeJournal article
CollectionUniversity of Macau
Affiliation1.Hong Kong University of Science and Technology
2.Shenzhen University
Recommended Citation
GB/T 7714
Fu L.,Zhai J.P.,Hu J.M.,et al. Synthesis of large silicon substituted AlPO4-11 single crystals[J]. Microporous and Mesoporous Materials,2011,137(1-3):1-7.
APA Fu L.,Zhai J.P.,Hu J.M.,Li I.L.,Ruan S.C.,&Tang Z.K..(2011).Synthesis of large silicon substituted AlPO4-11 single crystals.Microporous and Mesoporous Materials,137(1-3),1-7.
MLA Fu L.,et al."Synthesis of large silicon substituted AlPO4-11 single crystals".Microporous and Mesoporous Materials 137.1-3(2011):1-7.
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